2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

Base Information

Chemical Name:2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate
CAS No.:1156506-80-7
Molecular Formula:C₂₄H₁₉NO₄
Molecular Weight:385.419
Hs Code.:

Synonyms:2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

Suppliers and Price of 2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 6 raw suppliers

Chemical Property of 2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

Chemical Property:

Purity/Quality:: 99%, ^*data from raw suppliers

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Technology Process of 2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

There total 3 articles about 2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 5336-90-3
acridine-9-carboxylic acid

: 34137-14-9
methyl 4-hydroxy-3,5-dimethylbenzoate

: 1156506-80-7
2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

Guidance literature:: acridine-9-carboxylic acid; With pyridine; p-toluenesulfonyl chloride; Inert atmosphere;

methyl 4-hydroxy-3,5-dimethylbenzoate; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 1536146-87-8
2'-6'-dimethyl-4'-methoxycarbonylphenyl acridan-9-carboxylate

: sodium 3-bromopropane-1-sulfonate

: 1156506-80-7
2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

: 946423-59-2
2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate

Guidance literature:: 2'-6'-dimethyl-4'-methoxycarbonylphenyl acridan-9-carboxylate; sodium 3-bromopropane-1-sulfonate; With potassium carbonate; 1-butyl-3-methylimidazolium Tetrafluoroborate; at 160 - 165 ℃; for 3h; Inert atmosphere;

With oxygen; at 160 - 165 ℃; for 1h; Reagent/catalyst; Temperature; Time;

Reference yield:

: 4919-37-3
3,5-dimethyl-4-hydroxybenzoic acid

: 1156506-80-7
2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 16 h / 20 °C / Cooling with ice

2.1: pyridine; p-toluenesulfonyl chloride / Inert atmosphere

2.2: 16 h / 20 °C / Inert atmosphere

With pyridine; thionyl chloride; p-toluenesulfonyl chloride;