2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate

Base Information

• Chemical Name: 2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate
• CAS No.: 946423-59-2
• Molecular Formula: C₂₇H₂₅NO₇S
• Molecular Weight: 507.564
• Mol file: 946423-59-2.mol

Synonyms:2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate

Chemical Property of 2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate

There total 4 articles about 2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-propanesultone (1120-71-4) + 2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate (1156506-80-7) → 2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate (946423-59-2)

Guidance literature:

In N,N-dimethyl-formamide; at 155 ℃; for 6h; Product distribution / selectivity;

Reference yield:

2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate (1156506-80-7) + sodium 3-bromopropane-1-sulfonate → 2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate (946423-59-2)

Guidance literature:

With potassium carbonate; 1-butyl-3-methylimidazolium Tetrafluoroborate; at 160 - 165 ℃; for 3h; Reagent/catalyst; Inert atmosphere;

Reference yield:

2'-6'-dimethyl-4'-methoxycarbonylphenyl acridan-9-carboxylate (1536146-87-8) + sodium 3-bromopropane-1-sulfonate → 2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate (1156506-80-7) + 2'-6'-dimethyl-4'-methoxycarbonylphenyl 10-sulfopropylacridinium-9-carboxylate (946423-59-2)

Guidance literature:

2'-6'-dimethyl-4'-methoxycarbonylphenyl acridan-9-carboxylate; sodium 3-bromopropane-1-sulfonate; With potassium carbonate; 1-butyl-3-methylimidazolium Tetrafluoroborate; at 160 - 165 ℃; for 3h; Inert atmosphere;

With oxygen; at 160 - 165 ℃; for 1h; Reagent/catalyst; Temperature; Time;

upstream raw materials:

1,3-propanesultone

2',6'-dimethyl-4'-methoxycarbonylphenyl acridine-9-carboxylate

2'-6'-dimethyl-4'-methoxycarbonylphenyl acridan-9-carboxylate

Downstream raw materials:

2',6'-dimethyl-4'-carboxyphenyl-10-sulfopropylacridinium-9-carboxylate

C₃₁H₃₆N₃O₆S⁽¹⁺⁾

CN-NSP-DM AE-Z₃-NHS

C₄₃H₆₃N₆O₁₁S₃⁽¹⁺⁾