(S,R)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide

Base Information

• Chemical Name: (S,R)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide
• CAS No.: 1504566-94-2
• Molecular Formula: C₂₃H₂₀F₈N₄O₂S
• Molecular Weight: 568.491

Synonyms:(S,R)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide

Chemical Property of (S,R)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide

Chemical Property:

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Technology Process of (S,R)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide

There total 2 articles about (S,R)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N²-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N¹-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C22H20F8N2O2S + CYANAMID (420-04-2) → (S,R)-3-fluoro-N2-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N2-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide (1504566-94-2)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In acetonitrile; at 0 - 20 ℃; for 1.5h;

DOI:10.1021/jf501727k

Reference yield:

C12H12FNO2S → (S,R)-3-fluoro-N2-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N2-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide (1504566-94-2)

Guidance literature:

Multi-step reaction with 2 steps

2: [bis(acetoxy)iodo]benzene / acetonitrile / 1.5 h / 0 - 20 °C

With [bis(acetoxy)iodo]benzene; In acetonitrile;

DOI:10.1021/jf501727k

Reference yield:

(S,R)-3-fluoro-N2-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide or (S,S)-3-fluoro-N2-(1-(N-cyano-S-methylsulfinimidoyl)propan-2-yl)-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide (1504566-94-2) + trifluoroacetic anhydride (407-25-0) → 3-fluoro-N2-(1-(N-trifluoroacetyl-S-methylsulfinimidoyl)propan-2-yl)-N1-(2-methyl-4-(perfluoropropan-2-yl)phenyl)phthalamide

Guidance literature:

In dichloromethane; at 20 ℃; for 0.75h;

DOI:10.1021/jf503513n

upstream raw materials:

CYANAMID

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