N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

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Chemical Name:N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin
CAS No.:107222-72-0
Molecular Formula:C₄₉H₅₆N₄O₂₂
Molecular Weight:1053
Hs Code.:

N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

Synonyms:N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

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Chemical Property of N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

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Technology Process of N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

There total 3 articles about N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin-benzylester

: 107222-72-0
N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

Guidance literature:: With hydrogen; 10% palladium on active carbon; In ethyl acetate; for 2h;

Reference yield:

: 107222-69-5
N-(3,5-Dimethoxy-α,α-dimethylbenzyloxycarbonyl)-L-serin-benzylester

: 107222-72-0
N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) molecular sieve (4 Angstroem), drierite, Ag₂CO₃; 2.) AgClO₄ / 1.) CH₂Cl₂, toluene, 0 deg C, 0.5 h; CH₂Cl₂, toluene, 20 h

2: 93 percent / hydrogen / Pd/C (10percent Pd) / ethyl acetate / 2 h

With calcium sulfate; 4 A molecular sieve; hydrogen; silver perchlorate; silver carbonate; 10% palladium on active carbon; In ethyl acetate;

Reference yield:

: 96043-05-9
2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-β-D-galactopyranosylchlorid

: 107222-72-0
N-<2-Azido-4,6-di-O-benzoyl-2-desoxy-3-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-α-D-galactopyranosyloxycarbonyl>-O-(3,5-dimethoxy-α,α-dimethylbenzyl)-L-serin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) molecular sieve (4 Angstroem), drierite, Ag₂CO₃; 2.) AgClO₄ / 1.) CH₂Cl₂, toluene, 0 deg C, 0.5 h; CH₂Cl₂, toluene, 20 h

2: 93 percent / hydrogen / Pd/C (10percent Pd) / ethyl acetate / 2 h

With calcium sulfate; 4 A molecular sieve; hydrogen; silver perchlorate; silver carbonate; 10% palladium on active carbon; In ethyl acetate;