Cyclopropaneacetaldehyde, 2-(3-methoxyphenyl)-, (1R,2S)-rel- (9CI)

Base Information

Chemical Name:Cyclopropaneacetaldehyde, 2-(3-methoxyphenyl)-, (1R,2S)-rel- (9CI)
CAS No.:689258-86-4
Molecular Formula:C12H14O2
Molecular Weight:190.23836
Hs Code.:
Mol file:689258-86-4.mol

Synonyms:Cyclopropaneacetaldehyde, 2-(3-methoxyphenyl)-, (1R,2S)-rel- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclopropaneacetaldehyde, 2-(3-methoxyphenyl)-, (1R,2S)-rel- (9CI)

Chemical Property:

PSA：26.30000
LogP:2.38770

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclopropaneacetaldehyde, 2-(3-methoxyphenyl)-, (1R,2S)-rel- (9CI)

There total 6 articles about Cyclopropaneacetaldehyde, 2-(3-methoxyphenyl)-, (1R,2S)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 2-(3-methoxyphenyl)cyclopropanecarbaldehyde

: 4009-98-7
(methoxymethyl)triphenylphosphonium chloride

: 689258-86-4
[2-(3-methoxyphenyl)cyclopropyl]acetaldehyde

Guidance literature:: (methoxymethyl)triphenylphosphonium chloride; With lithium hexamethyldisilazane; In tetrahydrofuran; at 4 ℃; for 0.333333h;

2-(3-methoxyphenyl)cyclopropanecarbaldehyde; In tetrahydrofuran; at 4 - 20 ℃; for 1.5h;

With hydrogenchloride; water; In tetrahydrofuran; for 2h; Heating / reflux;

Reference yield:

: N-methoxy-2-(3-methoxyphenyl)-N-methylcyclopropanecarboxamide

: 689258-86-4
[2-(3-methoxyphenyl)cyclopropyl]acetaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: DIBAL

2.2: hydrochloric acid

With diisobutylaluminium hydride; 2.1: Wittig reaction;
DOI:10.1016/j.bmc.2007.03.020

Reference yield:

: 6099-04-3,17570-26-2
trans-3-methoxycinnamic acid

: 689258-86-4
[2-(3-methoxyphenyl)cyclopropyl]acetaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: 39 percent / 1-hydroxybenzotriazole hydrate; EDC; triethylamine

2.1: NaH

3.1: DIBAL

4.2: hydrochloric acid

With sodium hydride; diisobutylaluminium hydride; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 1-hydroxybenzotriazol-hydrate; triethylamine; 4.1: Wittig reaction;
DOI:10.1016/j.bmc.2007.03.020