Technology Process of N5-Benzoyl-N2-(phenylsulfonyl)-2,5-diaminophenol
There total 9 articles about N5-Benzoyl-N2-(phenylsulfonyl)-2,5-diaminophenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran;
at 25 ℃;
under 760 Torr;
DOI:10.1021/jo00291a059
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 85 percent / K2CO3, tetra-n-butylammonium iodide / acetone / 20 h / Heating
2: 69 percent / sodium dithionite / tetrahydrofuran; H2O / 24 h / Heating
3: 90 percent / K2CO3 / tetrahydrofuran / 0.17 h / 25 °C
4: 88 percent / trifluoroacetic acid (0.25 M in CH2Cl2) / CH2Cl2 / 0.5 h / 25 °C
5: 79 percent / pyridine / tetrahydrofuran / 20 h / Heating
6: 93 percent / lead tetraacetate / CHCl3 / 6 h / 25 °C
7: H2 / 10percent Pd/C / tetrahydrofuran / 25 °C / 760 Torr
With
pyridine; lead(IV) acetate; sodium dithionite; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; trifluoroacetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; chloroform; water; acetone;
DOI:10.1021/jo00291a059
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / K2CO3 / tetrahydrofuran / 0.17 h / 25 °C
2: 88 percent / trifluoroacetic acid (0.25 M in CH2Cl2) / CH2Cl2 / 0.5 h / 25 °C
3: 79 percent / pyridine / tetrahydrofuran / 20 h / Heating
4: 93 percent / lead tetraacetate / CHCl3 / 6 h / 25 °C
5: H2 / 10percent Pd/C / tetrahydrofuran / 25 °C / 760 Torr
With
pyridine; lead(IV) acetate; hydrogen; potassium carbonate; trifluoroacetic acid;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1021/jo00291a059
