4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin

Base Information

Chemical Name:4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin
CAS No.:942304-68-9
Molecular Formula:C₇₉H₉₇N₅O₂₄Si
Molecular Weight:1528.74
Hs Code.:

Synonyms:4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin

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Chemical Property of 4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin

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Technology Process of 4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin

There total 1 articles about 4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 942304-67-8
C₇₆H₉₃N₅O₂₄Si

: 556-56-9
allyl iodid

: 942304-68-9
4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at 20 ℃;
DOI:10.1021/jm061200+

Reference yield: 75.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 942304-68-9
4',6'-O-benzylidene-2''-O-allyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin

: 4',6'-O-benzylidene-2''-O-cinnamyl-5''-O-t-butyldimethylsilyl-penta-N-benzyloxycarbonyl paromomycin

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Heating;
DOI:10.1021/jm061200+