tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

Base Information

Chemical Name:tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside
CAS No.:1260145-60-5
Molecular Formula:C₆₉H₇₅N₇O₁₉Si
Molecular Weight:1334.48
Hs Code.:

tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

Synonyms:tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

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Chemical Property of tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

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Technology Process of tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

There total 1 articles about tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1260145-53-6
2,3,5,6-tetra-O-benzoyl-D-galactofuranoside N-phenyltrifluoroacetimidate

: 1260145-58-1
tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

: 1260145-60-5
tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja1087375

Reference yield:

: 1260145-60-5
tert-butyldimethylsilyl 3-O-acetyl-2-azido-4-(benzyloxycarbonyl)amino-2,4,6-trideoxy-α-D-galactopyranosyl-(1->4)-[2,3,5,6-tetra-O-benzoyl-β-D-galactofuranosyl-(1->3)]-2-azido-6-O-benzyl-2-deoxy-β-D-galactopyranoside

: C₆₃H₆₁N₇O₁₉

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja1087375