Technology Process of C22H14Cl3F7N4OS
There total 7 articles about C22H14Cl3F7N4OS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine;
In
ISOPROPYLAMIDE;
at 80 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / triphenylphosphine; palladium diacetate / Inert atmosphere; Reflux
2: potassium carbonate; methanol / tetrahydrofuran / 1 h
3: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h
4: water; lithium hydroxide / tetrahydrofuran / 15 h / 50 °C
5: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 80 °C
With
methanol; copper(ll) sulfate pentahydrate; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; potassium carbonate; sodium L-ascorbate; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
palladium diacetate; triphenylphosphine;
In
tetrahydrofuran; ISOPROPYLAMIDE; water; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium L-ascorbate; copper(ll) sulfate pentahydrate / water; tert-butyl alcohol / 96 h
2: water; lithium hydroxide / tetrahydrofuran / 15 h / 50 °C
3: bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine / ISOPROPYLAMIDE / 16 h / 80 °C
With
copper(ll) sulfate pentahydrate; water; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; ISOPROPYLAMIDE; water; tert-butyl alcohol;