2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene

Base Information

• Chemical Name: 2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene
• CAS No.: 1334128-68-5
• Molecular Formula: C₉H₂Cl₂F₇N₃
• Molecular Weight: 356.03

Synonyms:2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene

Chemical Property of 2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene

Chemical Property:

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Technology Process of 2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene

There total 2 articles about 2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-dichloro-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]aniline (273735-64-1) → 2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene (1334128-68-5)

Guidance literature:

2,6-dichloro-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]aniline; With hydrogenchloride; In water; tert-butyl alcohol; at 20 ℃; for 0.5h;

With sodium nitrite; In water; tert-butyl alcohol; at 0 - 5 ℃; for 1.5h;

With sodium azide; In water; tert-butyl alcohol; at 20 ℃;

Reference yield:

→ 2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene (1334128-68-5)

Guidance literature:

Reference yield:

2-chloro-5-ethynyl-benzoic acid methyl ester (792912-10-8) + 2-azido-1,3-dichloro-5-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]benzene (1334128-68-5) → methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate (1416900-81-6)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; for 96h;

upstream raw materials:

2,6-dichloro-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]aniline

Downstream raw materials:

methyl 2-chloro-5-{1-[2,6-dichloro-4-(1,1,1,2,3,3,3-heptafluoropropan-2-yl)phenyl]1H-1,2,3-triazol-4-yl}benzoate

2-chloro-5-{1-[2,6-dichloro-4-(1,2,2,2-tetrafluoro-1-trifluoromethyl-ethyl)-phenyl]-1H-[1,2,3]triazol-4-yl}-benzoic acid

2-chloro-N-cyclopropyl-5-{1-[2,6-dichloro-4-(1,2,2,2-tetrafluoro-1-trifluoromethyl-ethyl)phenyl]-1H-[1,2,3]triazol-4-yl}benzamide

C₂₂H₁₄Cl₃F₇N₄OS

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