benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester

Base Information

• Chemical Name: benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester
• CAS No.: 80977-16-8
• Molecular Formula: C₃₃H₃₁N₃O₈
• Molecular Weight: 597.624

Synonyms:benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester

Chemical Property of benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester

Chemical Property:

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Technology Process of benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester

There total 3 articles about benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyloxycarbonyl-O-benzyl-L-tyrosine (86827-18-1,92455-53-3,16677-29-5) → benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester (80977-16-8)

Guidance literature:

Multi-step reaction with 2 steps

1: N-methylmorpholine / acetonitrile / 0.17 h / -15 °C

2: N-methylmorpholine / acetonitrile

With 4-methyl-morpholine; In acetonitrile;

DOI:10.1071/CH9812439

Reference yield:

N-carbobenzoxy-β-alanine-p-nitrophenyl ester (3642-91-9) → benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester (80977-16-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / 2 M HBr in CH₃COOH / 1 h / Ambient temperature

2: N-methylmorpholine / acetonitrile

With 4-methyl-morpholine; hydrogen bromide; In acetonitrile;

DOI:10.1071/CH9812439

Reference yield:

β-alanine p-nitrophenyl ester hydrobromide (51165-88-9) + C29H31NO6 → benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanine p-nitrophenyl ester (80977-16-8)

Guidance literature:

With 4-methyl-morpholine; In acetonitrile; Yield given;

DOI:10.1071/CH9812439

upstream raw materials:

β-alanine p-nitrophenyl ester hydrobromide

N-carbobenzoxy-β-alanine-p-nitrophenyl ester

N-benzyloxycarbonyl-O-benzyl-L-tyrosine

Downstream raw materials:

benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanyl-L-phenylalanyl-L-leucine benzyl ester

(S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

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