(S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

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Chemical Name:(S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid
CAS No.:80977-36-2
Molecular Formula:C₂₇H₃₆N₄O₆
Molecular Weight:512.606
Hs Code.:

Synonyms:(S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

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Chemical Property of (S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

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Technology Process of (S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

There total 5 articles about (S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 80977-17-9
benzyloxycarbonyl-O-benzyl-L-tyrosyl-β-alanyl-L-phenylalanyl-L-leucine benzyl ester

: 80977-36-2
(S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; In methanol;
DOI:10.1071/CH9812439

Reference yield:

: 86827-18-1,92455-53-3,16677-29-5
N-benzyloxycarbonyl-O-benzyl-L-tyrosine

: 80977-36-2
(S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: N-methylmorpholine / acetonitrile / 0.17 h / -15 °C

2: N-methylmorpholine / acetonitrile

3: 98 percent / Et₃N / dimethylformamide / Ambient temperature

4: 95 percent / H₂, gl. CH₃COOH / 10percent Pd/C / methanol

With 4-methyl-morpholine; hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1071/CH9812439

Reference yield:

: 73994-87-3
(S)-benzyl 2-((S)-2-amino-3-phenylpropanamido)-4-methylpentanoate hydrochloride

: 80977-36-2
(S)-2-((S)-2-{3-[(S)-2-Amino-3-(4-hydroxy-phenyl)-propionylamino]-propionylamino}-3-phenyl-propionylamino)-4-methyl-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / dimethylformamide / Ambient temperature

2: 95 percent / H₂, gl. CH₃COOH / 10percent Pd/C / methanol

With hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In methanol; N,N-dimethyl-formamide;
DOI:10.1071/CH9812439