6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose

Base Information

Chemical Name:6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose
CAS No.:1632073-55-2
Molecular Formula:C₅₇H₆₉NO₁₂
Molecular Weight:960.174
Hs Code.:

Synonyms:6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose

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Chemical Property of 6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose

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Technology Process of 6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose

There total 6 articles about 6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 2,3,3’,4,4’-penta-O-benzyl-6,6’-bis-O-(2-methylsulfonyloxyethyl)-1’-O-(prop-2-en-1-yl)sucrose

: 109-85-3
2-methoxyethylamine

: 1632073-55-2
6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose

Guidance literature:: With sodium carbonate; potassium iodide; In acetonitrile; at 80 ℃;
DOI:10.1055/s-0033-1340180

Reference yield:

: 1632073-49-4
2,3,3’,4,4’-penta-O-benzyl-6-O-(2-tert-butoxy-2-oxoethyl)-1’-O-(prop-2-en-1-yl)sucrose

: 1632073-55-2
6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammomium bromide; sodium hydroxide / toluene / 10 h / 45 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / -78 - 20 °C

3: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 2 h / -78 - 20 °C

4: potassium iodide; sodium carbonate / acetonitrile / 80 °C

With dmap; lithium aluminium tetrahydride; tetrabutylammomium bromide; sodium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; sodium hydroxide; In tetrahydrofuran; dichloromethane; toluene; acetonitrile;
DOI:10.1055/s-0033-1340180

Reference yield:

: C₅₄H₆₄O₁₃

: 1632073-55-2
6,6’-(3-aza(2-methoxyethyl)penta-1,5-di-yl)-2,3,3’,4,4’-penta-O-benzyl-1’-O-(prop-2-en-1-yl)sucrose

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 2 h / -78 - 20 °C

2: potassium iodide; sodium carbonate / acetonitrile / 80 °C

With dmap; sodium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; In dichloromethane; acetonitrile;
DOI:10.1055/s-0033-1340180