2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole

Base Information

Chemical Name:2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole
CAS No.:1026948-54-8
Molecular Formula:C₂₉H₂₉NO₂Si
Molecular Weight:451.64
Hs Code.:

Synonyms:2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole

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Chemical Property of 2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole

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Technology Process of 2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole

There total 3 articles about 2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143215-88-7
1-<3-<(1,1-dimethylethyl)dimethylsiloxy>phenyl>-2-(4,5-diphenyl-2-oxazolyl)ethanone

: 1026948-54-8
2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole

Guidance literature:: With 3-ethyl-2-chlorobenzoxazolium tetrafluoroborate; triethylamine; In dichloromethane; at 0 - 20 ℃; for 17h;
DOI:10.1021/jm00097a006

Reference yield:

: 14224-99-8
2-methyl-4,5-diphenyloxazole

: 1026948-54-8
2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, -78 deg C, 30 min, 2.) THF, 1.5 h

2: Et₃N, 2-chloro-3-ethylbenzoxazolium tetrafluoroborate / CH₂Cl₂ / 17 h / 0 - 20 °C

With 3-ethyl-2-chlorobenzoxazolium tetrafluoroborate; triethylamine; lithium diisopropyl amide; In dichloromethane;
DOI:10.1021/jm00097a006

Reference yield:

: 120687-94-7
3-t-butyldimethylsilyloxybenzoic acid methyl ester

: 1026948-54-8
2-[3-(tert-Butyl-dimethyl-silanyloxy)-phenylethynyl]-4,5-diphenyl-oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) LDA / 1.) THF, -78 deg C, 30 min, 2.) THF, 1.5 h

2: Et₃N, 2-chloro-3-ethylbenzoxazolium tetrafluoroborate / CH₂Cl₂ / 17 h / 0 - 20 °C

With 3-ethyl-2-chlorobenzoxazolium tetrafluoroborate; triethylamine; lithium diisopropyl amide; In dichloromethane;
DOI:10.1021/jm00097a006