C₂₃H₂₇ClN₆O₃

Base Information

Chemical Name:C₂₃H₂₇ClN₆O₃
CAS No.:1094106-73-6
Molecular Formula:C₂₃H₂₇ClN₆O₃
Molecular Weight:470.959
Hs Code.:

C<sub>23</sub>H<sub>27</sub>ClN<sub>6</sub>O<sub>3</sub>

Synonyms:C₂₃H₂₇ClN₆O₃

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Chemical Property of C₂₃H₂₇ClN₆O₃

Chemical Property:

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Technology Process of C₂₃H₂₇ClN₆O₃

There total 8 articles about C₂₃H₂₇ClN₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1094106-57-6
2-(5-chloro-2-(1H-tetrazol-1-yl)phenyl)ethanamine

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1094106-73-6
C₂₃H₂₇ClN₆O₃

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 2.5 - 5h; Product distribution / selectivity;

Reference yield:

: C₁₂H₁₁ClN₄O₂

: 1094106-73-6
C₂₃H₂₇ClN₆O₃

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide; water / methanol / 20 °C

2: hydrogen; platinum(IV) oxide / methanol

3: triethylamine / tetrahydrofuran / -78 °C

4: ammonia / methanol

5: bis-[(trifluoroacetoxy)iodo]benzene; pyridine / acetonitrile; water

6: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With pyridine; platinum(IV) oxide; ammonia; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; bis-[(trifluoroacetoxy)iodo]benzene; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetonitrile; 5: |Hofmann Rearrangement;
DOI:10.1016/j.bmcl.2015.11.089

Reference yield:

: 942316-74-7
1-(4-chloro-2-iodophenyl)-1H-tetrazole

: 1094106-73-6
C₂₃H₂₇ClN₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine; palladium diacetate / acetonitrile / 24 h / 85 °C

2: sodium hydroxide; water / methanol / 20 °C

3: hydrogen; platinum(IV) oxide / methanol

4: triethylamine / tetrahydrofuran / -78 °C

5: ammonia / methanol

6: bis-[(trifluoroacetoxy)iodo]benzene; pyridine / acetonitrile; water

7: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide

With pyridine; platinum(IV) oxide; ammonia; water; hydrogen; palladium diacetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; bis-[(trifluoroacetoxy)iodo]benzene; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; acetonitrile; 1: |Heck Reaction / 6: |Hofmann Rearrangement;
DOI:10.1016/j.bmcl.2015.11.089