C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾
CAS No.:1234307-25-5
Molecular Formula:C₅₂H₉₄I₃O₁₂SSi₃*Na
Molecular Weight:1431.34
Hs Code.:

C<sub>52</sub>H<sub>94</sub>I<sub>3</sub>O<sub>12</sub>SSi<sub>3</sub><sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾

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Chemical Property of C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾

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Technology Process of C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾

There total 9 articles about C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1234307-24-4
C₅₄H₉₇I₃O₁₀SSi₃

: 1234307-25-5
C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾

Guidance literature:: With Oxone; potassium acetate; acetic acid; at 20 ℃; for 24h;

Reference yield:

: 7464-56-4,821794-45-0
1-O-allyl-α-D-glucopyranoside

: 1234307-25-5
C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 7 steps

1: dmap; pyridine / 16 h / 20 °C

2: 2,6-dimethylpyridine / dichloromethane / 16 h / Inert atmosphere

3: ethanol / 3 h / Reflux

4: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 22 h / 20 °C

5: pyridine / dichloromethane / 2 h / 20 °C

6: dmap; 2,2'-dipyridyl carbonate / dichloromethane / 48 h / 20 °C

7: Oxone; potassium acetate; acetic acid / 24 h / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; Oxone; 2,2'-dipyridyl carbonate; trimethylamine-N-oxide; water; potassium acetate; acetic acid; osmium(VIII) oxide; In ethanol; dichloromethane; tert-butyl alcohol;

Reference yield:

: 2280-44-6
D-Glucose

: 1234307-25-5
C₅₂H₉₄I₃O₁₂SSi₃^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 9 steps

1.1: trifluorormethanesulfonic acid / 48 h / 0 - 80 °C

1.2: 4 h / 40 °C

2.1: water; acetic acid / 1 h / 100 °C

3.1: dmap; pyridine / 16 h / 20 °C

4.1: 2,6-dimethylpyridine / dichloromethane / 16 h / Inert atmosphere

5.1: ethanol / 3 h / Reflux

6.1: trimethylamine-N-oxide; water / osmium(VIII) oxide / tert-butyl alcohol / 22 h / 20 °C

7.1: pyridine / dichloromethane / 2 h / 20 °C

8.1: dmap; 2,2'-dipyridyl carbonate / dichloromethane / 48 h / 20 °C

9.1: Oxone; potassium acetate; acetic acid / 24 h / 20 °C

With pyridine; 2,6-dimethylpyridine; dmap; Oxone; 2,2'-dipyridyl carbonate; trimethylamine-N-oxide; trifluorormethanesulfonic acid; water; potassium acetate; acetic acid; osmium(VIII) oxide; In ethanol; dichloromethane; tert-butyl alcohol;