Technology Process of C15H16O4S
There total 5 articles about C15H16O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap;
In
acetonitrile;
at 20 ℃;
for 17h;
Inert atmosphere;
DOI:10.3987/COM-12-S(N)91
- Guidance literature:
-
Multi-step reaction with 3 steps
1: [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride / tetrahydrofuran; hexane / 1 h / 0 - 60 °C / Inert atmosphere
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; aq. phosphate buffer / 1.75 h / 0 - 20 °C / Inert atmosphere
3: dmap / acetonitrile / 17 h / 20 °C / Inert atmosphere
With
dmap; [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; aq. phosphate buffer; hexane; dichloromethane; acetonitrile;
1: |Negishi Coupling;
DOI:10.3987/COM-12-S(N)91
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; aq. phosphate buffer / 1.75 h / 0 - 20 °C / Inert atmosphere
2: dmap / acetonitrile / 17 h / 20 °C / Inert atmosphere
With
dmap; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
aq. phosphate buffer; dichloromethane; acetonitrile;
DOI:10.3987/COM-12-S(N)91