C₂₄H₃₄O₃Si

Base Information

Chemical Name:C₂₄H₃₄O₃Si
CAS No.:1269618-61-2
Molecular Formula:C₂₄H₃₄O₃Si
Molecular Weight:398.618
Hs Code.:

C<sub>24</sub>H<sub>34</sub>O<sub>3</sub>Si

Synonyms:C₂₄H₃₄O₃Si

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Chemical Property of C₂₄H₃₄O₃Si

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Technology Process of C₂₄H₃₄O₃Si

There total 2 articles about C₂₄H₃₄O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1269618-60-1
C₂₅H₃₆O₂Si

: 1269618-61-2
C₂₄H₃₄O₃Si

Guidance literature:: C₂₅H₃₆O₂Si; With ozone; In dichloromethane; at -78 ℃;

With triphenylphosphine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/anie.201006780

Reference yield:

: 1269618-58-7
(3S,4R)-7-[(tert-butyldiphenyl)oxy]-3-methyl-hept-1-en-4-ol

: 1269618-61-2
C₂₄H₃₄O₃Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 - 20 °C / Inert atmosphere

2.1: ozone / dichloromethane / -78 °C

2.2: 1 h / 20 °C

With sodium hydride; ozone; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1002/anie.201006780

Reference yield:

: 1269618-61-2
C₂₄H₃₄O₃Si

: 1269618-49-6
C₂₇H₄₁O₆PSi

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 2.5 h / -78 °C / Inert atmosphere

1.3: Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

With n-butyllithium; Dess-Martin periodane; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/anie.201006780