5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II)

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Chemical Name:5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II)
CAS No.:1573176-52-9
Molecular Formula:C₁₅₀H₁₆₀N₁₂Ni₃Si₂
Molecular Weight:2363.24
Hs Code.:

Synonyms:5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II)

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Chemical Property of 5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II)

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Technology Process of 5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II)

There total 1 articles about 5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1573176-47-2
5,15-dibromo-10,20-bis(triisopropylsilylethynyl)porphyrin Ni(II)

: 1573176-69-8
5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-15-phenyl-10,20-bis(3,5-di-tert-butylphenyl)porphyrin Ni(II)

: 1573176-52-9
5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II)

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; triphenylphosphine; In water; N,N-dimethyl-formamide; toluene; at 100 ℃; for 3h; Schlenk technique; Inert atmosphere;
DOI:10.1021/ol500569b

Reference yield: 56.0%

: 1573176-52-9
5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II)

: 1573176-56-3
5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}porphyrin trisNi(II)

Guidance literature:: 5,15-bis{5,15-bis(3,5-di-tert-butylphenyl)-10-phenylporphyrin-20-yl}-10,20-bis(triisopropylsilylethynyl)porphyrin trisNi(II); With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -40 ℃; for 0.166667h; Schlenk technique; Inert atmosphere;

With para-dodecylbenzenesulfonic acid; In water; 1,2-dichloro-ethane; at 80 ℃; for 29h;
DOI:10.1021/ol500569b