Cbz-GlyAib₈OtBu

Base Information

Chemical Name:Cbz-GlyAib₈OtBu
CAS No.:1219615-82-3
Molecular Formula:C₄₆H₇₅N₉O₁₂
Molecular Weight:946.155
Hs Code.:

Synonyms:Cbz-GlyAib₈OtBu

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Chemical Property of Cbz-GlyAib₈OtBu

Chemical Property:

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Technology Process of Cbz-GlyAib₈OtBu

There total 5 articles about Cbz-GlyAib₈OtBu which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1130642-54-4
H-Aib₈OtBu

: 1138-80-3
N-(Benzyloxycarbonyl)glycine

: 1219615-82-3
Cbz-GlyAib₈OtBu

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 48h;
DOI:10.1002/bip.21535

Reference yield:

: 1187839-02-6
N₃(α-aminoisobutyric acid)₄OtBu

: 1219615-82-3
Cbz-GlyAib₈OtBu

Guidance literature:: Multi-step reaction with 4 steps

1.1: palladium on activated charcoal; hydrogen / ethanol

2.1: acetic anhydride / 2 h / 120 °C

2.2: Reflux

3.1: palladium on activated charcoal; hydrogen / ethanol

4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 48 h

With palladium on activated charcoal; hydrogen; acetic anhydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane;
DOI:10.1002/bip.21535

Reference yield:

: 1219615-78-7
N₃Aib₈OtBu

: 1219615-82-3
Cbz-GlyAib₈OtBu

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal; hydrogen / ethanol

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 48 h

With palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane;
DOI:10.1002/bip.21535