Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(NC₅H₄)C₂₀H₈N₂C₄C₂₀H₈N₄(C₅H₄N)(C₆H₄(OCH₂CH₂)3OMe)2)

Base Information

Chemical Name:Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(NC₅H₄)C₂₀H₈N₂C₄C₂₀H₈N₄(C₅H₄N)(C₆H₄(OCH₂CH₂)3OMe)2)
CAS No.:1062503-93-8
Molecular Formula:C₁₀₆H₁₀₀N₁₀O₁₆Zn₂
Molecular Weight:1900.8
Hs Code.:

Zn<sub>2</sub>((MeO(CH<sub>2</sub>CH<sub>2</sub>O)3C<sub>6</sub>H<sub>4</sub>)2(NC<sub>5</sub>H<sub>4</sub>)C<sub>20</sub>H<sub>8</sub>N<sub>2</sub>C<sub>4</sub>C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>5</sub>H<sub>4</sub>N)(C<sub>6</sub>H<sub>4</sub>(OCH<sub>2</sub>CH<sub>2</sub>)3OMe)2)

Synonyms:Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(NC₅H₄)C₂₀H₈N₂C₄C₂₀H₈N₄(C₅H₄N)(C₆H₄(OCH₂CH₂)3OMe)2)

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Chemical Property of Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(NC₅H₄)C₂₀H₈N₂C₄C₂₀H₈N₄(C₅H₄N)(C₆H₄(OCH₂CH₂)3OMe)2)

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Technology Process of Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(NC₅H₄)C₂₀H₈N₂C₄C₂₀H₈N₄(C₅H₄N)(C₆H₄(OCH₂CH₂)3OMe)2)

There total 2 articles about Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(NC₅H₄)C₂₀H₈N₂C₄C₂₀H₈N₄(C₅H₄N)(C₆H₄(OCH₂CH₂)3OMe)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1051971-74-4
C₉₆H₉₂Br₂N₈O₁₆Zn₂

: 1692-15-5
4-pyridylboronic acid

: 1062503-93-8
C₁₀₆H₁₀₀N₁₀O₁₆Zn₂

Guidance literature:: C₉₆H₉₂Br₂N₈O₁₆Zn₂; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; at 20 ℃; for 0.25h;

4-pyridylboronic acid; With sodium hydrogencarbonate; In tetrahydrofuran; 1,2-dimethoxyethane; water; at 20 - 70 ℃;

Reference yield: 52.0%

: 1051971-74-4
Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(Br)C₂₀H₈N₂C₄C₂₀H₈N₄(Br)(C₆H₄(OCH₂CH₂)3OMe)2)

: 1692-15-5
4-pyridylboronic acid

: 1062503-93-8
Zn₂((MeO(CH₂CH₂O)3C₆H₄)2(NC₅H₄)C₂₀H₈N₂C₄C₂₀H₈N₄(C₅H₄N)(C₆H₄(OCH₂CH₂)3OMe)2)

Guidance literature:: With sodium hydrogencarbonate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; water; (Ar); stirring. mixt. of porphyrin deriv. and palladium compd. in DME and THF at room temp. for 15 min, addn. of boronic acid deriv., NaHCO3, water and THF, heating at 70°C overnight; cooling, filtration through celite with THF, chromy. (CH2Cl2/methanol/pyridine (97.5:2.5:1)), ppn. by layering DME soln. with pentane, NMR and MALDI;
DOI:10.1039/b814789b