1-(3-Bromobenzoyl)piperidine

Base Information

Chemical Name:1-(3-Bromobenzoyl)piperidine
CAS No.:59507-53-8
Molecular Formula:C12H14BrNO
Molecular Weight:268.153
Hs Code.:2933399090
DSSTox Substance ID:DTXSID20354936
Nikkaji Number:J3.588.413K
Wikidata:Q82133444
Mol file:59507-53-8.mol

Synonyms:1-(3-Bromobenzoyl)piperidine;59507-53-8;(3-bromophenyl)(piperidin-1-yl)methanone;(3-bromophenyl)-piperidin-1-ylmethanone;(3-bromophenylcarbonyl)piperidine;CBMicro_012453;Cambridge id 5157026;SCHEMBL18734295;DTXSID20354936;SMSF0003970;MFCD00194116;STK408030;AKOS000179269;CB15654;SB43894;BS-28976;BIM-0012160.P001;CS-0207019;A869185;SR-01000197283;SR-01000197283-1;Z27689079

Suppliers and Price of 1-(3-Bromobenzoyl)piperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Oakwood
1-(3-Bromobenzoyl)piperidine 98%
25g
$ 270.00

Crysdot
(3-Bromophenyl)(piperidin-1-yl)methanone 95+%
100g
$ 677.00

Chemenu
(3-Bromophenyl)(piperidin-1-yl)methanone 95%
100g
$ 640.00

ChemBridge Corporation
1-(3-bromobenzoyl)piperidine 95%
5 g
$ 133.00

ChemBridge Corporation
1-(3-bromobenzoyl)piperidine 95%
1 g
$ 46.00

American Custom Chemicals Corporation
1-(3-BROMOBENZOYL)PIPERIDINE 95.00%
1G
$ 679.37

American Custom Chemicals Corporation
1-(3-BROMOBENZOYL)PIPERIDINE 95.00%
5G
$ 1107.30

Alichem
(3-Bromophenyl)(piperidin-1-yl)methanone
100g
$ 718.20

AK Scientific
1-(3-Bromobenzoyl)piperidine
5g
$ 171.00

Total 10 raw suppliers

Chemical Property of 1-(3-Bromobenzoyl)piperidine

Chemical Property:

Vapor Pressure:5.67E-06mmHg at 25°C
Refractive Index:1.585
Boiling Point:379.9°C at 760 mmHg
Flash Point:183.5°C
PSA：20.31000
Density:1.406g/cm³
LogP:3.01310
Storage Temp.:2-8°C
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:267.02588
Heavy Atom Count:15
Complexity:226

Purity/Quality:

97% ^*data from raw suppliers

1-(3-Bromobenzoyl)piperidine 98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCN(CC1)C(=O)C2=CC(=CC=C2)Br

Technology Process of 1-(3-Bromobenzoyl)piperidine

There total 6 articles about 1-(3-Bromobenzoyl)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110-89-4
piperidine

: 3132-99-8
m-bromobenzoic aldehyde

: 59507-53-8
(3-bromophenyl)(piperidin-1-yl)methanone

Guidance literature:: With tert.-butylhydroperoxide; In 1,4-dioxane; at 60 ℃; for 8h; Inert atmosphere;
DOI:10.1002/cctc.202001041

Reference yield: 88.0%

: 110-89-4
piperidine

: 585-76-2
m-bromobenzoic acid

: 59507-53-8
(3-bromophenyl)(piperidin-1-yl)methanone

Guidance literature:: m-bromobenzoic acid; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

piperidine; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/jm5002277

Reference yield: 75.0%

: 110-89-4
piperidine

: 591-18-4
1-Bromo-3-iodobenzene

: 201230-82-2
carbon monoxide

: 59507-53-8
(3-bromophenyl)(piperidin-1-yl)methanone

Guidance literature:: With palladium diacetate; potassium carbonate; In glycerol; at 60 ℃; for 3h; under 20521.4 Torr; Solvent; chemoselective reaction; Autoclave; Green chemistry;
DOI:10.1039/c8cc03858a