2-benzyloxybutyric acid ethyl ester

Base Information

Chemical Name:2-benzyloxybutyric acid ethyl ester
CAS No.:110298-79-8
Molecular Formula:C₁₃H₁₈O₃
Molecular Weight:222.284
Hs Code.:

Synonyms:2-benzyloxybutyric acid ethyl ester

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Chemical Property of 2-benzyloxybutyric acid ethyl ester

Chemical Property:

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Technology Process of 2-benzyloxybutyric acid ethyl ester

There total 2 articles about 2-benzyloxybutyric acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 533-68-6
2-bromobutyric acid ethyl ester

: 110298-79-8
2-benzyloxybutyric acid ethyl ester

Guidance literature:: benzyl alcohol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

2-bromobutyric acid ethyl ester; In tetrahydrofuran; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.12.011

Reference yield:

: 110298-79-8
2-benzyloxybutyric acid ethyl ester

: 110298-79-8,110351-29-6,137169-32-5
(R)-2-Benzyloxy-butyric acid ethyl ester

: 110351-29-6
(S)-2-Benzyloxy-butyric acid ethyl ester

Guidance literature:: With diammonium phosphate; manganese(II) sulfate; yeast ext; magnesium sulfate; iron(II) sulfate; zinc(II) sulfate; In water; at 30 ℃; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; suspension of grown cells of Corynebacterium equi IFO 3730, pH = 7.2, e.e. = 77percent;
DOI:10.1016/S0040-4039(00)95353-X

Reference yield: 85.0%

: 110298-79-8
2-benzyloxybutyric acid ethyl ester

: 137169-33-6
(3R)-benzyloxybutanoic acid

Guidance literature:: 2-benzyloxybutyric acid ethyl ester; With lithium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 16.5h;

With hydrogenchloride; In tetrahydrofuran; diethyl ether; water; pH=4;
DOI:10.1016/j.tetlet.2011.12.011