3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide

Base Information

Chemical Name:3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide
CAS No.:1609184-89-5
Molecular Formula:C₃₀H₃₂N₆O₆
Molecular Weight:572.621
Hs Code.:

Synonyms:3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide

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Chemical Property of 3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide

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Technology Process of 3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide

There total 2 articles about 3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyiodomethyl-β-D-galactopyranosyl azide

: 1609184-89-5
3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 24h; stereoselective reaction;
DOI:10.1016/j.carres.2014.02.022

Reference yield:

: 710965-73-4
(1S,3R,4R,5R,6S,7S)-4,5-Bis-benzyloxy-3-benzyloxymethyl-2-oxa-bicyclo[4.1.0]heptane-7-carboxylic acid methyl ester

: 1609184-89-5
3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; N-iodo-succinimide / acetonitrile / 12 h / 20 °C / Molecular sieve; Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C

With N-iodo-succinimide; sodium azide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2014.02.022

Reference yield: 56.0%

: 1609184-89-5
3,4,6-tri-O-benzyl-2-deoxy-2-C-carbmethoxyazidomethyl-β-D-galactopyranosyl azide

: 1609184-90-8
(3S)-3-amino-(3,4,6-tri-O-benzyl-1,2-dideoxy-α-D-galactopyranoso)[2,3-b]-pyrrolidin-2-one

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 25 ℃; for 12h; stereoselective reaction;
DOI:10.1016/j.carres.2014.02.022