methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate

Base Information

• Chemical Name: methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate
• CAS No.: 910875-08-0
• Molecular Formula: C₁₇H₂₇BO₄Si
• Molecular Weight: 334.295

Synonyms:methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate

Chemical Property of methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate

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Technology Process of methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate

There total 3 articles about methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

methyl coumalate (6018-41-3) + 4,4,5,5-tetramethyl-2-trimethylsilanylethynyl-[1,3,2]dioxaborolane (159087-46-4) → methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)benzoate (910875-11-5) + methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate (910875-08-0)

Guidance literature:

In 1,2-dichloro-benzene; at 180 ℃; for 18h;

DOI:10.1016/j.tet.2007.08.118

Reference yield:

methyl 2-pyrone-4-carboxylate (59776-81-7) + 2-ethynyl-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane (347389-74-6) → methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)benzoate (910875-11-5) + methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate (910875-08-0)

Guidance literature:

In 1,2-dichloro-benzene; at 180 ℃; for 15h;

DOI:10.1016/j.tet.2007.08.118

Reference yield:

methyl 2-pyrone-4-carboxylate (59776-81-7) + 4,4,5,5-tetramethyl-2-trimethylsilanylethynyl-[1,3,2]dioxaborolane (159087-46-4) → methyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-4-(trimethylsilyl)benzoate (910875-11-5) + methyl 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(trimethylsilyl)benzoate (910875-08-0)

Guidance literature:

at 170 ℃; for 15h;

DOI:10.1039/b607322k

upstream raw materials:

methyl coumalate

4,4,5,5-tetramethyl-2-trimethylsilanylethynyl-[1,3,2]dioxaborolane

methyl 2-pyrone-4-carboxylate

2-ethynyl-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

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