(Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

Base Information

Chemical Name:(Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide
CAS No.:1560811-12-2
Molecular Formula:C₁₅H₁₉F₃INOS
Molecular Weight:445.288
Hs Code.:

Synonyms:(Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

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Technology Process of (Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

There total 1 articles about (Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 875446-23-4
2-iodo-5-(trifluoromethyl)benzaldehyde

: 18925-10-5
allylzinc bromide

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 1560811-12-2
(Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

Guidance literature:: 2-iodo-5-(trifluoromethyl)benzaldehyde; (R)-2-methylpropane-2-sulfinamide; With titanium(IV) tetraethanolate; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;

allylzinc bromide; In tetrahydrofuran; at -60 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol500142c

Reference yield: 70.0%

: 1560811-12-2
(Rs)-N-((S)-1-(2-iodo-5-(trifluoromethyl)phenyl)but-3-en-1-yl)-2-methylpropane-2-sulfinamide

: 536-74-3
phenylacetylene

: 1560811-30-4
(Rs)-2-methyl-N-((S)-1-(2-(phenylethynyl)-5-(trifluoromethyl)phenyl)but-3-en-1-yl)propane-2-sulfinamide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; triethylamine; at 65 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol500142c