bis(mesitylenesulfonyl) ester of 1,4-butanediol

Base Information

• Chemical Name: bis(mesitylenesulfonyl) ester of 1,4-butanediol
• CAS No.: 328260-27-1
• Molecular Formula: C₂₂H₃₀O₆S₂
• Molecular Weight: 454.609

Synonyms:bis(mesitylenesulfonyl) ester of 1,4-butanediol

Chemical Property of bis(mesitylenesulfonyl) ester of 1,4-butanediol

Chemical Property:

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Technology Process of bis(mesitylenesulfonyl) ester of 1,4-butanediol

There total 1 articles about bis(mesitylenesulfonyl) ester of 1,4-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

2-mesitylenesulphonyl chloride (773-64-8) + Butane-1,4-diol (110-63-4) → bis(mesitylenesulfonyl) ester of 1,4-butanediol (328260-27-1)

Guidance literature:

With potassium hydroxide; benzyltriethylammonium bromide; In 1,4-dioxane; at 5 ℃; for 4h;

DOI:10.1021/jm000309t

Reference yield: 93.0%

bis(mesitylenesulfonyl) ester of 1,4-butanediol (328260-27-1) + N-ethyl N,N'-bis(mesitylenesulfonyl)-trans-1,2-bis(aminomethyl)cyclopropane → C54H78N4O8S4

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; for 10h;

DOI:10.1021/jm030175u

Reference yield: 42.0%

bis(mesitylenesulfonyl) ester of 1,4-butanediol (328260-27-1) + N1,N4-bis(mesitylenesulfonyl)-N4-ethyl-1,4-diamino-2-butene (304862-42-8) → (Z,Z)-3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaeicosa-5,10-diene (328260-29-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 5 ℃; for 4h;

DOI:10.1021/jm000309t

upstream raw materials:

2-mesitylenesulphonyl chloride

Butane-1,4-diol

Downstream raw materials:

(Z,Z)-3,8,13,18-tetrakis(mesitylenesulfonyl)-3,8,13,18-tetraazaeicosa-5,10-diene

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