3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

Base Information

Chemical Name:3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane
CAS No.:959935-47-8
Molecular Formula:C₂₃H₂₈Br₄
Molecular Weight:624.091
Hs Code.:

Synonyms:3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

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Chemical Property of 3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

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Technology Process of 3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

There total 3 articles about 3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 733-07-3
dimesitylmethane

: 959935-47-8
3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

Guidance literature:: With hydrogen bromide; acetic acid; at 95 ℃; for 12h;
DOI:10.1039/c2dt12427k

Reference yield: 76.0%

: 913724-94-4
3,3'-bis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 959935-47-8
3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

Guidance literature:: formaldehyd; With hydrogen bromide; zinc dibromide; In acetic acid; at 100 ℃; for 0.5h;

3,3'-bis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane; In acetic acid; at 100 ℃; for 8h;
DOI:10.1039/b901173k

Reference yield:

: 108-67-8
1,3,5-trimethyl-benzene

: 959935-47-8
3,3',5,5'-tetrakis(bromomethyl)-2,2',4,4',6,6'-hexamethyldiphenylmethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: formic acid / 80 °C

1.2: 6 h / Reflux

2.1: acetic acid; hydrogen bromide / 12 h / 95 °C

With formic acid; hydrogen bromide; acetic acid;
DOI:10.1039/c3cc46613b