1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester

Base Information

• Chemical Name: 1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester
• CAS No.: 108931-51-7
• Molecular Formula: C₁₇H₂₁N₃O₅
• Molecular Weight: 347.371

Synonyms:1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester

Chemical Property of 1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester

Chemical Property:

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Technology Process of 1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester

There total 1 articles about 1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O-methylisourea hemisulfate (29427-58-5,24285-39-0) + 2-[(3-nitrophenyl)methylene]-3-oxobutanoic acid,1,1-dimethylethyl ester (103295-96-1) → 1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester (108931-51-7)

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 65 ℃;

Reference yield:

phosgene (75-44-5) + aqueous dimethylamine + 1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester (108931-51-7) → 3-[(dimethylamino)carbonyl]-1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxo-5-pyrimidinecarboxylic acid, t-butyl ester

Guidance literature:

With hydrogenchloride; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; benzene;

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 1,4-dihydro-2-methoxy-6-methyl-4-(3-nitrophenyl)-5-pyrimidinecarboxylic acid,1,1-dimethylethyl ester (108931-51-7) → 3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5(2H)-pyrimidinedicarboxylic acid, bis(1,1-dimethylethyl) ester (108930-66-1)

Guidance literature:

With hydrogenchloride; dmap; In acetonitrile;

upstream raw materials:

O-methylisourea hemisulfate

2-[(3-nitrophenyl)methylene]-3-oxobutanoic acid,1,1-dimethylethyl ester

Downstream raw materials:

tert-butyl 6-methyl-4-(3-nitrophenyl)-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

3,6-dihydro-4-methyl-6-(3-nitrophenyl)-2-oxo-1,5(2H)-pyrimidinedicarboxylic acid, bis(1,1-dimethylethyl) ester

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