2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

Base Information

Chemical Name:2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone
CAS No.:929048-42-0
Molecular Formula:C₂₃H₂₉NO₆
Molecular Weight:415.486
Hs Code.:

Synonyms:2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

Suppliers and Price of 2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

There total 7 articles about 2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 929048-89-5
2-(3,4,5-trimethoxyphenyl)-2-acetoxy-N-methyl-N-(2-isopropoxy-3-methoxybenzyl)-acetamide

: 929048-42-0
2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 6h; Heating / reflux;

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 929048-42-0
2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-benzyl-N,N,N-triethylammonium chloride / dichloromethane; water / 2 h / 0 - 20 °C

2.1: hydrogenchloride / methanol / 2.83 h / 15 - 20 °C

2.2: 2 h

3.1: 3 h / 20 °C

4.1: 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 20 °C / Heating / reflux

4.2: 2 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane / 6 h / Heating / reflux

With hydrogenchloride; 1,1'-carbonyldiimidazole; trifluoroacetic acid; N-benzyl-N,N,N-triethylammonium chloride; In methanol; dichloromethane; water;

Reference yield:

: 75792-35-7
2-isopropoxy-3-methoxy-benzaldehyde

: 929048-42-0
2-methyl-4-(3,4,5-trimethoxyphenyl)-8-isopropoxy-7-methoxy-1,4-dihydro-3(2H)-isoquinolinone

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / methanol / 20 h / 20 °C / Molecular sieve

1.2: 1 h / 0 - 20 °C

2.1: 1,1'-carbonyldiimidazole / dichloromethane / 1 h / 20 °C / Heating / reflux

2.2: 2 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 6 h / Heating / reflux

With sodium hydroxide; 1,1'-carbonyldiimidazole; trifluoroacetic acid; In methanol; dichloromethane;