(S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester

Base Information

Chemical Name:(S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester
CAS No.:323592-89-8
Molecular Formula:C₂₂H₃₄N₂O₅
Molecular Weight:406.522
Hs Code.:

Synonyms:(S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester

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Chemical Property of (S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester

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Technology Process of (S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester

There total 2 articles about (S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6436-90-4
ethyl 2-(benzylamino)acetate

: 102308-32-7
(4S)-4-formyl-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 323592-89-8
(S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester

Guidance literature:: With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol; at 20 ℃; for 18h;
DOI:10.1021/ol048235t

Reference yield:

: 95715-86-9,108149-60-6
(S)-2,2-dimethyl-oxazolidine-3,4-dicarboxylic acid 3-tert-butyl ester 4-methyl ester

: 323592-89-8
(S)-4-formyl-2,2-dimethyl-3-oxazolidinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: DIBAL-H / toluene / 0.5 h / -78 °C

2: 16.83 g / AcOH; NaBH₃CN / methanol; tetrahydrofuran / 18 h / 20 °C

With diisobutylaluminium hydride; sodium cyanoborohydride; acetic acid; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/ol048235t