methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside
CAS No.:118088-83-8
Molecular Formula:C₃₆H₄₅NO₁₁
Molecular Weight:667.753
Hs Code.:

Synonyms:methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

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Chemical Property of methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

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Technology Process of methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

There total 4 articles about methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 118088-82-7
methyl 4-O-(2-acetamido-3,4,6-tri-O-benzoyl-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 118088-83-8
methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; for 20h; Ambient temperature;
DOI:10.1246/bcsj.61.1291

Reference yield:

: 82469-72-5
3,4,6-tri-O-benzoyl-2-(benzoyloximino)-2-deoxy-α-D-arabino-hexopyranosyl bromide

: 118088-83-8
methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / silver carbonate, iodine, molecular sieve 3A / CH₂Cl₂ / 48 h / Ambient temperature; in the dark

2: 1 M diborane / tetrahydrofuran / -10 deg C, 0.5 h; room temperature, 2 h

3: 411 mg / tetrahydrofuran; methanol / 1 h / Ambient temperature

4: 87 percent / 0.05 M sodium methoxide / methanol / 20 h / Ambient temperature

With 3 A molecular sieve; iodine; sodium methylate; silver carbonate; diborane; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1246/bcsj.61.1291

Reference yield:

: C₅₅H₅₅NO₁₃

: 118088-83-8
methyl 4-O-(2-acetamido-2-deoxy-β-D-mannopyranosyl)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 411 mg / tetrahydrofuran; methanol / 1 h / Ambient temperature

2: 87 percent / 0.05 M sodium methoxide / methanol / 20 h / Ambient temperature

With sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1246/bcsj.61.1291