2,4-DINITRO-2'-METHYLDIPHENYLAMINE

Base Information

• Chemical Name: 2,4-DINITRO-2'-METHYLDIPHENYLAMINE
• CAS No.: 964-75-0
• Molecular Formula: C₁₃H₁₁N₃O₄
• Molecular Weight: 273.248
• Mol file: 964-75-0.mol

Synonyms:2,4-dinitro-N-o-tolylaniline

Chemical Property of 2,4-DINITRO-2'-METHYLDIPHENYLAMINE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

2,4-DINITRO-2'-METHYLDIPHENYLAMINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-DINITRO-2'-METHYLDIPHENYLAMINE

There total 5 articles about 2,4-DINITRO-2'-METHYLDIPHENYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

meta-dinitrobenzene (99-65-0) + o-toluidine (95-53-4) → 2,4-dinitro-N-o-tolylaniline (964-75-0)

Guidance literature:

o-toluidine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - -70 ℃; Inert atmosphere;

meta-dinitrobenzene; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.3998/ark.5550190.0012.917

Reference yield:

1-chloro-2,4-dinitro-benzene (97-00-7) + o-toluidine (95-53-4) → 2,4-dinitro-N-o-tolylaniline (964-75-0)

Guidance literature:

With zinc(II) chloride;

Reference yield:

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + o-toluidine (95-53-4) → 2,4-dinitro-N-o-tolylaniline (964-75-0)

Guidance literature:

In dimethyl sulfoxide; at 30 ℃; F KIE;

DOI:10.1021/jo981301i

upstream raw materials:

1-chloro-2,4-dinitro-benzene

o-toluidine

2-nitro-benzenesulfonic acid-(2,4-dinitro-phenyl ester)

2,4-Dinitrofluorobenzene

Downstream raw materials:

4-nitro-N¹-o-tolyl-o-phenylenediamine

(2,4-dinitro-phenyl)-(2-methyl-4-nitro-phenyl)-amine

5-nitro-1-o-tolyl-1H-benzo[d][1,2,3]triazole