Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate

Base Information

Chemical Name:Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate
CAS No.:166818-15-1
Molecular Formula:C₁₇H₁₆I₃NO₇
Molecular Weight:727.03
Hs Code.:

Synonyms:Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate

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Chemical Property of Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate

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Technology Process of Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate

There total 3 articles about Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1185-59-7
tetraethylammonium acetate

: 166818-09-3
Dimethyl 2,4,6-triiodo-5-<2-(iodomethyl)-5-oxo-1-pyrrolidinyl>-1,3-benzenedicarboxylate

: 166818-15-1
Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate

Guidance literature:: In 1,4-dioxane; Heating;
DOI:10.1021/jo00119a020

Reference yield:

: 39716-58-0
pent-4-enoyl chloride

: 166818-15-1
Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / N,N-dimethyl-acetamide / 1.) 5 deg C, 0.5 h, 2.) room temp., 20 h

2: 86 percent / 5 M aq. NaOH, N-iodosuccinimide / methanol; dioxane

3: 77 percent / dioxane / Heating

With sodium hydroxide; N-iodo-succinimide; In 1,4-dioxane; methanol; N,N-dimethyl acetamide;
DOI:10.1021/jo00119a020

Reference yield:

: 166818-05-9
Dimethyl 2,4,6-triiodo-5-<(1-oxo-4-pentenoyl)amino>-1,3-benzenedicarboxylate

: 166818-15-1
Dimethyl 5-<2-<(acetyloxy)methyl>-5-oxo-1-pyrrolidinyl>-2,4,6-triiodo-1,3-benzenedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / 5 M aq. NaOH, N-iodosuccinimide / methanol; dioxane

2: 77 percent / dioxane / Heating

With sodium hydroxide; N-iodo-succinimide; In 1,4-dioxane; methanol;
DOI:10.1021/jo00119a020