[(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)]

Base Information

Chemical Name:[(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)]
CAS No.:927674-68-8
Molecular Formula:C₃₅H₅₁Cl₂N₃O₂Th
Molecular Weight:848.753
Hs Code.:

[(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl<sub>2</sub>(dme)]

Synonyms:[(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)]

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Chemical Property of [(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)]

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Technology Process of [(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)]

There total 2 articles about [(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 639084-65-4
[ThCl₄(1,2-dimethoxyethane)₂]

: 184640-73-1
2,6-bis(2,6-bis((2,6-diisopropylphenyl)amino)methyl)pyridine

: 927674-68-8
[(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)]

Guidance literature:: With LiCH₂SiMe₃; In toluene; Sonication; under Ar atm. TlCl4(dme)2 and LiCH2SiMe3 in toluene were stirred for 1 hat -78°C followed by 1 h at 0°C, soln. ligand in toluene was added dropwise, allowed to warm to room temp. and stirred for 12 h; soln. was filtered, solvent was removed in vacuo, hexane was added, followed by sonication and filtration;
DOI:10.1021/om060914f

Reference yield: 51.0%

: 639084-65-4
[ThCl₄(1,2-dimethoxyethane)₂]

: Li₂[2,6-bis(2,6-diisopropylanilidomethyl)pyridine]

: 927674-68-8
[(2,6-bis(2,6-diisopropylanilidomethyl)pyridine)ThCl₂(dme)]

Guidance literature:: In benzene; Sonication; under Ar atm. to soln. TlCl4(dme)2 in benzene in ice-water bath soln. Lisalt ligand in benzene was added dropwise and stirred for 1 h; soln. was filtered, solvent was removed in vacuo, hexane was added, followed by sonication and filtration;
DOI:10.1021/om060914f