C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)

Base Information

Chemical Name:C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)
CAS No.:1419176-84-3
Molecular Formula:C₂₂H₂₁N₂*F₆P
Molecular Weight:458.386
Hs Code.:

C<sub>22</sub>H<sub>21</sub>N<sub>2</sub><sup>(1+)</sup>*F<sub>6</sub>P<sup>(1-)</sup>

Synonyms:C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)

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Chemical Property of C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)

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Technology Process of C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)

There total 3 articles about C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1419176-81-0
C₂₂H₂₁N₂⁽¹⁺⁾*Br^(1-)

: 1419176-84-3
C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)

Guidance literature:: With ammonium hexafluorophosphate; In water; at 0 ℃; for 0.25h; Inert atmosphere; Schlenk technique;
DOI:10.1021/om301152n

Reference yield:

: 4403-69-4
2-amino-1-benzylamine

: 1419176-84-3
C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)

Guidance literature:: Multi-step reaction with 3 steps

1.1: 13 h / 130 - 150 °C / Inert atmosphere; Schlenk technique

2.1: potassium tert-butylate / acetonitrile / Inert atmosphere; Schlenk technique

2.2: 4 h / 90 °C / Inert atmosphere; Schlenk technique

3.1: ammonium hexafluorophosphate / water / 0.25 h / 0 °C / Inert atmosphere; Schlenk technique

With ammonium hexafluorophosphate; potassium tert-butylate; In water; acetonitrile;
DOI:10.1021/om301152n

Reference yield:

: 1904-64-9
3,4-dihydroquinazoline

: 1419176-84-3
C₂₂H₂₁N₂⁽¹⁺⁾*F₆P^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / acetonitrile / Inert atmosphere; Schlenk technique

1.2: 4 h / 90 °C / Inert atmosphere; Schlenk technique

2.1: ammonium hexafluorophosphate / water / 0.25 h / 0 °C / Inert atmosphere; Schlenk technique

With ammonium hexafluorophosphate; potassium tert-butylate; In water; acetonitrile;
DOI:10.1021/om301152n