4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

Base Information

Chemical Name:4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)
CAS No.:108053-97-0
Molecular Formula:C₁₇H₁₈Cl₄N₂O₂
Molecular Weight:424.154
Hs Code.:

Synonyms:4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

Suppliers and Price of 4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

Chemical Property:

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Technology Process of 4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

There total 3 articles about 4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108053-96-9
4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzoic acid)

: 108053-97-0
4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 4h; Heating;

Reference yield:

: 18711-13-2
4,7-dichloroisatin

: 108053-97-0
4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) dioxan, 60 deg C, 30 min, 2.) dioxan, DMSO, 100 deg C, 30 min

2: 1.) 2.5 M aq. NaOH, 2.) 5percent H₂O₂ / 2.) 3 h

3: 75 percent / LiAlH₄ / diethyl ether / 4 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; dihydrogen peroxide; sodium hydride; In diethyl ether;

Reference yield:

: 108053-95-8
4,4',7,7'-tetrachloro-1,1'-(propane-1,3-diyl)bis(2,3-dihydroindole-2,3-dione)

: 108053-97-0
4,4',7,7'-tetrachloro-2,2'-(propane-1,3-diyldiimino)bis(benzyl alcohol)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 2.5 M aq. NaOH, 2.) 5percent H₂O₂ / 2.) 3 h

2: 75 percent / LiAlH₄ / diethyl ether / 4 h / Heating

With sodium hydroxide; lithium aluminium tetrahydride; dihydrogen peroxide; In diethyl ether;