Technology Process of C25H38OS2
There total 4 articles about C25H38OS2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H36O;
With
sodium hydride;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
carbon disulfide;
In
tetrahydrofuran;
for 2h;
Heating;
methyl iodide;
In
tetrahydrofuran;
for 0.75h;
Further stages.;
Heating;
DOI:10.1139/V07-091
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: t-BuLi / diethyl ether; pentane / -78 - 20 °C
1.2: 55 percent / AlMe3 / diethyl ether; pentane; hexane / -78 - 20 °C
2.1: NaH / tetrahydrofuran / 1 h / 0 °C
2.2: tetrahydrofuran / 2 h / Heating
2.3: 85 percent / tetrahydrofuran / 0.75 h / Heating
With
tert.-butyl lithium; sodium hydride;
In
tetrahydrofuran; diethyl ether; pentane;
DOI:10.1139/V07-091
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: BHBr2*SMe2 / CH2Cl2 / 20 °C
1.2: NaOH / CH2Cl2; H2O / 2.5 h / 20 °C
1.3: 84 percent / I2 / CH2Cl2; H2O / 2 h / 0 - 20 °C
2.1: t-BuLi / diethyl ether; pentane / -78 - 20 °C
2.2: 55 percent / AlMe3 / diethyl ether; pentane; hexane / -78 - 20 °C
3.1: NaH / tetrahydrofuran / 1 h / 0 °C
3.2: tetrahydrofuran / 2 h / Heating
3.3: 85 percent / tetrahydrofuran / 0.75 h / Heating
With
dibromoborane dimethylsulfide; tert.-butyl lithium; sodium hydride;
In
tetrahydrofuran; diethyl ether; dichloromethane; pentane;
DOI:10.1139/V07-091
