(1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester

Base Information

Chemical Name:(1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester
CAS No.:1342302-05-9
Molecular Formula:C₂₀H₂₇NO₄
Molecular Weight:345.439
Hs Code.:

Synonyms:(1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester

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Chemical Property of (1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester

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Technology Process of (1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester

There total 5 articles about (1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1342302-22-0
C₂₀H₂₉NO₄

: 1342302-05-9
(1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester

Guidance literature:: With Dess-Martin periodane; triethylamine; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1055/s-0030-1260102

Reference yield:

: 932743-56-1
(6S)-6-(4-methoxybenzylamino)cyclohex-1-enecarboxylic acid methyl ester

: 1342302-05-9
(1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; sodium iodide / acetonitrile / 0 - 20 °C

2: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C

3: Dess-Martin periodane; triethylamine / dichloromethane / 4 h / 20 °C

With diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; sodium iodide; In hexane; dichloromethane; acetonitrile; 3: Dess-Martin oxidation;
DOI:10.1055/s-0030-1260102

Reference yield:

: 1342302-04-8
(6S)-6-[tert-butoxycarbonyl-(4-methoxybenzyl)amino]cyclohex-1-enecarboxylic acid methyl ester

: 1342302-05-9
(1S)-(2-formylcyclohex-2-enyl)(4-methoxybenzyl)carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / hexane; dichloromethane / 0.5 h / -78 °C

2: Dess-Martin periodane; triethylamine / dichloromethane / 4 h / 20 °C

With diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; In hexane; dichloromethane; 2: Dess-Martin oxidation;
DOI:10.1055/s-0030-1260102