2-Piperazinecarboxylicacid,1,4-dimethyl-3,6-dioxo-(9CI)

Base Information

• Chemical Name: 2-Piperazinecarboxylicacid,1,4-dimethyl-3,6-dioxo-(9CI)
• CAS No.: 519141-05-0
• Molecular Formula: C7H10N2O4
• Molecular Weight: 186.167
• Mol file: 519141-05-0.mol

Synonyms:2-Piperazinecarboxylicacid,1,4-dimethyl-3,6-dioxo-(9CI);1,4-DIMETHYL-3,6-DIOXOPIPERAZINE-2-CARBOXYLIC ACID

Chemical Property of 2-Piperazinecarboxylicacid,1,4-dimethyl-3,6-dioxo-(9CI)

Chemical Property:

• PSA: 77.92000
• LogP: -1.75420

Purity/Quality:

1,4-dimethyl-3,6-dioxo-2-Piperazinecarboxylicacid 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Piperazinecarboxylicacid,1,4-dimethyl-3,6-dioxo-(9CI)

There total 2 articles about 2-Piperazinecarboxylicacid,1,4-dimethyl-3,6-dioxo-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-benzyloxycarbonyl-1,4-dimethylpiperazine-2,5-dione (519141-04-9) → sarcosine anhydride (5076-82-4) + 3-carboxyl-1,4-dimethylpiperazine-2,5-dione (519141-05-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; for 1h; Title compound not separated from byproducts;

DOI:10.1016/j.tet.2005.06.084

Reference yield:

3-(ethoxycarbonyl)-1,4-dimethylpiperazine-2,5-dione (865879-15-8) → sarcosine anhydride (5076-82-4) + 3-carboxyl-1,4-dimethylpiperazine-2,5-dione (519141-05-0)

Guidance literature:

With potassium hydroxide; In ethanol; water;

DOI:10.1016/j.tet.2005.06.084

Reference yield:

3-carboxyl-1,4-dimethylpiperazine-2,5-dione (519141-05-0) → sarcosine anhydride (5076-82-4)

Guidance literature:

Heating;

DOI:10.1016/S0040-4039(02)02571-6

upstream raw materials:

3-(ethoxycarbonyl)-1,4-dimethylpiperazine-2,5-dione

3-benzyloxycarbonyl-1,4-dimethylpiperazine-2,5-dione

Downstream raw materials:

sarcosine anhydride

3-allyl-1,4-dimethylpiperazine-2,5-dione

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