2,5-Piperazinedione,1,4-dimethyl-3-(2-propenyl)-(9CI)

Base Information

Chemical Name:2,5-Piperazinedione,1,4-dimethyl-3-(2-propenyl)-(9CI)
CAS No.:519141-21-0
Molecular Formula:C9H14N2O2
Molecular Weight:182.22
Hs Code.:
Mol file:519141-21-0.mol

Synonyms:2,5-Piperazinedione,1,4-dimethyl-3-(2-propenyl)-(9CI);1,4-DIMETHYL-3-(2-PROPENYL)-2,5-PIPERAZINEDIONE

Suppliers and Price of 2,5-Piperazinedione,1,4-dimethyl-3-(2-propenyl)-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
1,4-dimethyl-3-(2-propen-1-yl)-2,5-Piperazinedione 97.00%
25G
$ 18200.00

AccelPharmtech
1,4-dimethyl-3-(2-propen-1-yl)-2,5-Piperazinedione 97.00%
5G
$ 9620.00

AccelPharmtech
1,4-dimethyl-3-(2-propen-1-yl)-2,5-Piperazinedione 97.00%
1G
$ 5550.00

Total 1 raw suppliers

Chemical Property of 2,5-Piperazinedione,1,4-dimethyl-3-(2-propenyl)-(9CI)

Chemical Property:

PSA：40.62000
LogP:-0.26270

Purity/Quality:: 1,4-dimethyl-3-(2-propen-1-yl)-2,5-Piperazinedione 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,5-Piperazinedione,1,4-dimethyl-3-(2-propenyl)-(9CI)

There total 6 articles about 2,5-Piperazinedione,1,4-dimethyl-3-(2-propenyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 78877-99-3
3-methoxy-1,4-dimethylpiperazine-2,5-dione

: 762-72-1
allyl-trimethyl-silane

: 519141-21-0
3-allyl-1,4-dimethylpiperazine-2,5-dione

Guidance literature:: With boron trifluoride diethyl etherate;
DOI:10.1016/S0040-4039(02)02571-6

Reference yield:

: 519141-04-9
3-benzyloxycarbonyl-1,4-dimethylpiperazine-2,5-dione

: 519141-21-0
3-allyl-1,4-dimethylpiperazine-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂ / Pd/C / methanol / 1 h

2.1: I₂; diacetoxyiodobenzene / CH₂Cl₂ / 0.02 h

2.2: 76 percent / CH₂Cl₂ / 16 h

3.1: 68 percent / BF₃*OEt₂ / CH₂Cl₂ / 24 h / 20 °C

With [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; hydrogen; iodine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/j.tet.2005.06.084

Reference yield:

: 865879-15-8
3-(ethoxycarbonyl)-1,4-dimethylpiperazine-2,5-dione

: 519141-21-0
3-allyl-1,4-dimethylpiperazine-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: KOH / H₂O; ethanol

2.1: I₂; diacetoxyiodobenzene / CH₂Cl₂ / 0.02 h

2.2: 76 percent / CH₂Cl₂ / 16 h

3.1: 68 percent / BF₃*OEt₂ / CH₂Cl₂ / 24 h / 20 °C

With potassium hydroxide; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; iodine; In ethanol; dichloromethane; water;
DOI:10.1016/j.tet.2005.06.084