N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide

Base Information

Chemical Name:N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide
CAS No.:1428548-67-7
Molecular Formula:C₂₆H₂₃N₃O₃
Molecular Weight:425.487
Hs Code.:

Synonyms:N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide

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Chemical Property of N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide

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Technology Process of N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide

There total 3 articles about N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 117-34-0
2,2-diphenylacetic acid

: 1428548-66-6
5-amino-2-((benzyloxy)methyl)pyrimidin-4-ol

: 1428548-67-7
N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 1428548-65-5
2-((benzyloxy)methyl)-5-nitropyrimidin-4-ol

: 1428548-67-7
N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dithionite; water / tetrahydrofuran / 4 h / 20 °C

2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With sodium dithionite; water; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 133915-07-8
2-(benzyloxy)acetimidamide

: 1428548-67-7
N-(2-((benzyloxy)methyl)-4-hydroxypyrimidin-5-yl)-2,2-diphenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 30 °C

2: sodium dithionite; water / tetrahydrofuran / 4 h / 20 °C

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

With sodium dithionite; water; sodium methylate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;