4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile

Base Information

• Chemical Name: 4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile
• CAS No.: 1469858-24-9
• Molecular Formula: C₂₇H₂₇N₃OSSi
• Molecular Weight: 469.682

Synonyms:4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile

Chemical Property of 4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile

Chemical Property:

Purity/Quality:

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Technology Process of 4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile

There total 6 articles about 4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

6-(4-bromophenyl)-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene (1469858-10-3) + 4-cyanophenylboronic acid (126747-14-6) → 4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile (1469858-24-9)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In ethanol; toluene; at 100 ℃; for 8h;

Reference yield:

5,6-dihydro-<6H>-cyclopenta--thiophene-4-one (5650-51-1) → 4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile (1469858-24-9)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 6 h / 100 °C

2: hydrazine hydrate; acetic acid / ethanol / 4 h / 100 °C / Inert atmosphere

3: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

4: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; sodium hydride; sodium carbonate; hydrazine hydrate; acetic acid; In tetrahydrofuran; ethanol; toluene; mineral oil;

Reference yield:

6-(4-bromophenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene (1469857-12-2) → 4'-[4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl]biphenyl-4-carbonitrile (1469858-24-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 80 °C

2: sodium carbonate; bis-triphenylphosphine-palladium(II) chloride / ethanol; toluene / 8 h / 100 °C

With bis-triphenylphosphine-palladium(II) chloride; sodium hydride; sodium carbonate; In tetrahydrofuran; ethanol; toluene; mineral oil;

upstream raw materials:

6-(4-bromophenyl)-4-(2-trimethylsilanylethoxymethyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

4-cyanophenylboronic acid

6-(4-bromophenyl)-4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalene

5,6-dihydro-<6H>-cyclopenta--thiophene-4-one

Downstream raw materials:

4'-(4,7-dihydro-1-thia-4,5-diazacyclopenta[a]pentalen-6-yl)biphenyl-4-carbonitrile

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