(S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide

Base Information

Chemical Name:(S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide
CAS No.:791074-28-7
Molecular Formula:C₁₆H₂₃NO₄
Molecular Weight:293.363
Hs Code.:

Synonyms:(S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide

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Technology Process of (S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide

There total 6 articles about (S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7322-88-5
(S)-acetylmandelic acid

: 112245-13-3
(S)-tert-leucinol

: 791074-28-7
(S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide

Guidance literature:: (S)-acetylmandelic acid; With thionyl chloride; In dichloromethane; for 3h; Reflux;

(S)-tert-leucinol; With triethylamine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/acscatal.8b03170

Reference yield:

: 17199-29-0
(S)-Mandelic acid

: 112245-13-3
(S)-tert-leucinol

: 75-36-5
acetyl chloride

: 791074-28-7
(S,S)-O-acetylmandelic acid (1-hydroxymethyl-2,2-dimethyl)propylamide

Guidance literature:: (S)-Mandelic acid; acetyl chloride; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

With thionyl chloride; In dichloromethane; for 3h; Inert atmosphere; Schlenk technique; Reflux;

(S)-tert-leucinol; With triethylamine; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acscatal.9b01166