cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane

Base Information

Chemical Name:cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane
CAS No.:1260177-90-9
Molecular Formula:C₃₃H₂₁F₁₈N₃
Molecular Weight:801.521
Hs Code.:

Synonyms:cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane

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Technology Process of cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane

There total 1 articles about cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 401-95-6
3,5-Bis(trifluoromethyl)benzaldehyde

: 26150-46-9
cis,cis-1,3,5-triaminocyclohexane

: 1260177-90-9
cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane

Guidance literature:: With sodium hydroxide; In water; toluene; at 150 ℃;
DOI:10.1039/c0dt00986e

Reference yield: 92.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 1260177-90-9
cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)-benzylideneamino)cyclohexane

: [Cu(I)(cis,cis-1,3,5-tris(3,5-bis(trifluoromethyl)benzylideneamino)cyclohexane)(acetonitrile)]PF₆

Guidance literature:: In dichloromethane; byproducts: CH3CN; (inert atm.); addn. of CH2Cl2 soln. of 1 equiv. of copper compd. to CH2Cl2 soln. of trisimino deriv., stirring for 0.5 h at room temp.; addn. of hexane, filtration, drying in vac., elem. anal.;
DOI:10.1039/c0dt00986e