Technology Process of C29H46O6
There total 5 articles about C29H46O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C11H20O3;
With
triethylamine; (-)-diisopinocamphenylborane chloride;
In
diethyl ether;
at 0 ℃;
for 1h;
C18H26O3;
In
diethyl ether;
at -78 - -20 ℃;
for 18h;
optical yield given as %de;
DOI:10.1021/ol201426c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Hoveyda-Grubbs catalyst second generation / toluene / 18 h / 25 °C / Reflux
2.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / 0 °C
2.2: 18 h / -78 - -20 °C
With
Hoveyda-Grubbs catalyst second generation; triethylamine; (-)-diisopinocamphenylborane chloride;
In
diethyl ether; toluene;
2.2: Aldol condensation;
DOI:10.1021/ol201426c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetrahydrofuran; diethyl ether / -78 - 0 °C
2.1: triethylamine; (-)-diisopinocamphenylborane chloride / diethyl ether / 1 h / 0 °C
2.2: 18 h / -78 - -20 °C
With
triethylamine; (-)-diisopinocamphenylborane chloride;
In
tetrahydrofuran; diethyl ether;
2.2: Aldol condensation;
DOI:10.1021/ol201426c