2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate
CAS No.:146919-08-6
Molecular Formula:C₂₉H₂₉Cl₃N₄O₅
Molecular Weight:619.932
Hs Code.:

Synonyms:2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

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Technology Process of 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

There total 1 articles about 2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 2-azido-3,4,6-tri-O-benzyl-2-deoxy-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 146919-08-6
2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With potassium carbonate; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1016/0008-6215(95)00012-I

Reference yield: 51.0%

: 21862-63-5
trans-4-tert-butylcyclohexanol

: 146919-08-6
2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

: trans-4-tert-butylcyclohexyl-2-azido-2-deoxy-3,4,6-tri-O-benzyl-β-D-glucopyranoside

: trans-4-tert-butylcyclohexyl-2-azido-2-deoxy-3,4,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -25 ℃; for 1h;
DOI:10.1002/chem.200400746

Reference yield: 47.0%

: 868055-19-0
2-azido-1,3,5,6-tetra-O-benzyl-2-deoxy-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-D-mannitol

: 146919-08-6
2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl trichloroacetimidate

: 2-azido-1,3,5,6-tetra-O-benzyl-2-deoxy-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-α-D-glucopyranosyl)-D-mannitol

: 2-azido-1,3,5,6-tetra-O-benzyl-2-deoxy-4-O-(2-azido-3,6-di-O-benzyl-2-deoxy-4-O-(2-azido-3,4,6-tri-O-benzyl-2-deoxy-α-D-glucopyranosyl)-α-D-glucopyranosyl)-D-mannitol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In toluene; at -25 ℃; for 1.5h;
DOI:10.1039/b507824e