Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester

Base Information

Chemical Name:Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester
CAS No.:637338-47-7
Molecular Formula:C₂₉H₃₂N₂O₅
Molecular Weight:488.583
Hs Code.:

Synonyms:Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester

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Chemical Property of Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester

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Technology Process of Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester

There total 5 articles about Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 637338-43-3
Acetic acid (2S,3S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-6-naphthalen-1-yl-3,4-dihydro-2H-pyran-3-ylmethyl ester

: 637338-47-7
Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester

Guidance literature:: Acetic acid (2S,3S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-6-naphthalen-1-yl-3,4-dihydro-2H-pyran-3-ylmethyl ester; With borane-THF; In tetrahydrofuran; at 20 ℃; for 2h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; Heating;
DOI:10.1055/s-2003-40352

Reference yield:

: 22422-69-1
1-(naphthalen-1-yl)prop-2-en-1-one

: 637338-47-7
Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 9-BBN / tetrahydrofuran / 1 h / 20 °C

1.2: 73 percent / aq. H₂O₂; NaOH / tetrahydrofuran / 3 h / Heating

2.1: 80 percent / pyridine / 12 h / 0 - 20 °C

3.1: BH₃*THF / tetrahydrofuran / 2 h / 20 °C

3.2: 74 percent / aq. H₂O₂; NaOH / tetrahydrofuran / Heating

With pyridine; 9-borabicyclo[3.3.1]nonane dimer; borane-THF; In tetrahydrofuran;
DOI:10.1055/s-2003-40352

Reference yield:

: 92720-98-4
N-allenyl-N'-methyl-4-phenyl-5-methyl-2-imidazolidinone

: 637338-47-7
Acetic acid (2S,3S,5R,6S)-2-((4S,5R)-3,4-dimethyl-2-oxo-5-phenyl-imidazolidin-1-yl)-5-hydroxy-6-naphthalen-1-yl-tetrahydro-pyran-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 9-BBN / tetrahydrofuran / 1 h / 20 °C

1.2: 73 percent / aq. H₂O₂; NaOH / tetrahydrofuran / 3 h / Heating

2.1: 80 percent / pyridine / 12 h / 0 - 20 °C

3.1: BH₃*THF / tetrahydrofuran / 2 h / 20 °C

3.2: 74 percent / aq. H₂O₂; NaOH / tetrahydrofuran / Heating

With pyridine; 9-borabicyclo[3.3.1]nonane dimer; borane-THF; In tetrahydrofuran;
DOI:10.1055/s-2003-40352