Technology Process of 4-iodo-3-nitrobenzoyl chloride
There total 5 articles about 4-iodo-3-nitrobenzoyl chloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: chromium(VI) oxide; periodic acid; oxygen / acetonitrile / 60 °C / 760.05 Torr / Schlenk technique
2: thionyl chloride / toluene; tetrahydrofuran / 2 h / 80 °C / Schlenk technique; Inert atmosphere
With
chromium(VI) oxide; thionyl chloride; oxygen; periodic acid;
In
tetrahydrofuran; toluene; acetonitrile;
DOI:10.1039/c8ob01095a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: silver sulfate; copper diacetate; sodium iodide; 2.9-dimethyl-1,10-phenanthroline; oxygen / dimethyl sulfoxide / 20 h / 160 °C / 760.05 Torr / Schlenk technique
2: chromium(VI) oxide; periodic acid; oxygen / acetonitrile / 60 °C / 760.05 Torr / Schlenk technique
3: thionyl chloride / toluene; tetrahydrofuran / 2 h / 80 °C / Schlenk technique; Inert atmosphere
With
chromium(VI) oxide; thionyl chloride; 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; periodic acid; sodium iodide;
In
tetrahydrofuran; dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1039/c8ob01095a
