C₄₈H₅₀N₄O₁₂BCl₄I

Base Information

Chemical Name:C₄₈H₅₀N₄O₁₂BCl₄I
CAS No.:943975-91-5
Molecular Formula:C₄₈H₅₀BCl₄IN₄O₁₂
Molecular Weight:1154.47
Hs Code.:

C<sub>48</sub>H<sub>50</sub>N<sub>4</sub>O<sub>12</sub>BCl<sub>4</sub>I

Synonyms:C₄₈H₅₀N₄O₁₂BCl₄I

Suppliers and Price of C₄₈H₅₀N₄O₁₂BCl₄I

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₈H₅₀N₄O₁₂BCl₄I

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₈H₅₀N₄O₁₂BCl₄I

There total 21 articles about C₄₈H₅₀N₄O₁₂BCl₄I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 854443-88-2
2-[2-(3,5-dichloro-4-hydroxy-phenyl)-2-oxo-acetylamino]-3-[6-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-1H-indol-3-yl]-propionic acid

: C₂₃H₂₇N₂O₆Cl₂I

: 943975-91-5
C₄₈H₅₀N₄O₁₂BCl₄I

Guidance literature:: With 2,5-dimethylpyridine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; dichloromethane; at 5 ℃; for 12h;
DOI:10.1021/ol070889p

Reference yield:

: 943975-95-9
3,4-diisopropoxy-5-iodobenzaldehyde

: 943975-91-5
C₄₈H₅₀N₄O₁₂BCl₄I

Guidance literature:: Multi-step reaction with 10 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.75 h / -20 °C

1.2: 84 percent / tetrahydrofuran; hexane / 2.5 h / 20 °C

2.1: AD-mix-α / 2-methyl-propan-2-ol; H2O / 6 h / 25 °C

2.2: imidazole / dimethylformamide / 5 h / 0 °C

2.3: triphenylphosphine; diisopropyl azodicarboxylate; diphenylphosphoryl azide / tetrahydrofuran / 2 h / 0 °C

3.1: triphenylphosphine / tetrahydrofuran; H₂O / 3 h / 60 °C

4.1: Et₃N / CH₂Cl₂ / 20 °C

5.1: n-Bu₄NF / tetrahydrofuran / 2 h / 0 °C

6.1: aq. NaHCO₃; KBr; NaOCl / TEMPO / acetone / 1.5 h / 0 °C

7.1: SOCl₂ / 12 h / 20 °C

8.1: 80 percent / 2,5-lutidine; HATU / tetrahydrofuran; CH₂Cl₂ / 12 h / 5 °C

9.1: TFA / CH₂Cl₂ / 1 h / 0 °C

10.1: 78 percent / 2,5-lutidine; HATU / tetrahydrofuran; CH₂Cl₂ / 12 h / 5 °C

With sodium hypochlorite; AD-mix-α; n-butyllithium; thionyl chloride; 2,5-dimethylpyridine; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In tetrahydrofuran; hexane; dichloromethane; water; acetone; tert-butyl alcohol; 2.1: Sharpless asymmetric dihydroxylation / 2.3: Mitsunobu reaction;
DOI:10.1021/ol070889p

Reference yield:

: 943975-97-1
C₂₀H₃₄IO₃SiN₃

: 943975-91-5
C₄₈H₅₀N₄O₁₂BCl₄I

Guidance literature:: Multi-step reaction with 8 steps

1: triphenylphosphine / tetrahydrofuran; H₂O / 3 h / 60 °C

2: Et₃N / CH₂Cl₂ / 20 °C

3: n-Bu₄NF / tetrahydrofuran / 2 h / 0 °C

4: aq. NaHCO₃; KBr; NaOCl / TEMPO / acetone / 1.5 h / 0 °C

5: SOCl₂ / 12 h / 20 °C

6: 80 percent / 2,5-lutidine; HATU / tetrahydrofuran; CH₂Cl₂ / 12 h / 5 °C

7: TFA / CH₂Cl₂ / 1 h / 0 °C

8: 78 percent / 2,5-lutidine; HATU / tetrahydrofuran; CH₂Cl₂ / 12 h / 5 °C

With sodium hypochlorite; thionyl chloride; 2,5-dimethylpyridine; tetrabutyl ammonium fluoride; sodium hydrogencarbonate; triethylamine; triphenylphosphine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/ol070889p